Download PDF by Y. Mastai : Advances in Crystallization Processes

By Y. Mastai

ISBN-10: 9535105817

ISBN-13: 9789535105817

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Műszaki Szemle, 2007, 39-40, 48 [16] a). : J. Chem. Soc. Perkin Trans 2, 1994, 1883 b). : J. Therm. Anal. 1997, 48, 691. : Tetrahedron Lett. 1980, 21, 647. [19] Pasteur, L. Acad. , 1848, 26, 535. : Termal. Anal. 1988, 33, 1241. : J. Chem. Soc. Perkin Trans 2, 2000, 149. : Tetrahedron: Asymm. 2000, 11, 809. ; Simon, H;. : Chirality 2001, 13, 29. : PhD disz. 2003 [25] a). ; Fogassy, E. b). Hung. Pat. no. ; Böcskei, Zs. Chirality, 1994, 6, 314 [27] Kassai, Cs: PhD diss. : Tetrahedron Letters, 1994, 35, 257260 .

The obtained crystalline diastereoisomeric salt also will be a quasi-racemate, but its enantiomeric excess (ee: 93%) was even higher than that of the former case. It was also observed, that the average ee and F values of diastereoisomeric salts obtained at the resolutions (in number 28 resolutions) of racemic N-acetyl-phenylalanine and phenylglycine (AcPA and AcPG) with structurally similar bases (resolving agents) correspond to the eutectic composition (eeE value) of the adequate racemate (in these cases the enantiomers of the racemic compounds form racemates).

Chem. Soc. Perkin Trans. 2. 1988, 1385-1392. Hung. Pat. 255. ; Reck, G. J. Chem. Soc. Perkin Trans. , 1990, 1395. Hung. Pat. no. 866, 1985. :Hung. : Pat. No. WO 8503932, 1985, CAN 104:168835. ; Hirayama, N. Tetrahedron: Asymmetry, 2003, 14, 3716. ; Sakai, K. Tetrahedron: Asymmetry, 2003, 14, 411. ; Hirayama, N. Tetrahedron: Asymmetry, 2004, 15, 1073. ; Fogassy, E. Tetrahedron: Asymmetry, 2001, 12, 3435. ; Faigl, F. Tetrahedron, 1985, 41, 2465. ; Fogassy, E. Synth. , 1999, 29, 4315. [52] Hung. Pat.

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Advances in Crystallization Processes by Y. Mastai


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